Inhalt

[ 290CTPEBOTP19 ] PR Basic Lab Course in Organic Technology

Versionsauswahl
Workload Education level Study areas Responsible person Hours per week Coordinating university
2 ECTS B3 - Bachelor's programme 3. year Chemistry Klaus Bretterbauer 2 hpw Johannes Kepler University Linz
Detailed information
Pre-requisites PR Lab Course in Preparative Organic Chemistry 1 VL Instrumental Analytical Chemistry
or admission to the master's program for Chemistry and Chemical Technology
Original study plan Bachelor's programme Chemistry and Chemical Technology 2025W
Learning Outcomes
Competences
Students will be able to perform fundamental organic-technical experiments integrating sustainability, safety, and industrial practices.
Skills Knowledge
More specifically, upon completion of the course, they will be able to: • Carry out fundamental industrially relevant organic synthesis procedures following reported literature procedures on a multi-gram laboratory scale. (k3, k6) • Purify and isolate the targeted compound using industrially approved isolation and purification methods such as distillation, (bed)filtration, and crystallization. (k3, k4) • Assess and evaluate sustainability aspects of materials and industrially relevant organic synthesis procedures. (k2, k4, k5) • Assess and evaluate safety-relevant aspects of materials and industrially relevant organic synthesis procedures. (k2, k4, k5) • Apply the safety-relevant aspects to the execution of industrially relevant synthesis processes and the handling of hazardous materials. (k2, k3, k6) • Characterize and analyze organic-technical products by refractive index, melting point, spectroscopic means, (gas chromatography-mass spectrometry, Fourier-transform infrared spectroscopy), thermal analyses (thermogravimetric analysis, differential scanning calorimetry), and application-related testing. (k3, k4, k5) • Document their laboratory work in a protocol in a scientific writing style. (k4, k5) The course is divided into three consecutive sections devoted to the following experimental manipulations and industrially-relevant products: • Preparation, separation, purification, characterization, and application-related testing of biodiesel based on renewable resources (e.g., fats and oils). • Preparation, separation, purification, characterization, and application-related testing of surface-active substances based on renewable resources (e.g., fats and oils) and fossil-based feedstocks. • Perform reactions that include challenges in terms of kinetics and reaction energy employing differently controlled radical polymerizations.
Criteria for evaluation In the frame of interim evaluations, the practical work in the lab and a final exam.
Methods Practical work in the lab under guidance of supervisors.
Language English
Study material The descriptions of the experiments and the relevant theoretical backgrounds is available for download, secured by a password.
Changing subject? No
Further information The number of participants is limited.
Corresponding lecture in collaboration with 491CTOMAOTP19: PR Lab Course in Advanced Organic Technology (5 ECTS) equivalent to
491CTOSPTOP10: PR Praktikum aus Chemischer Technologie Organischer Stoffe (8,4 ECTS)
On-site course
Maximum number of participants 10
Assignment procedure Direct assignment