Inhalt

[ 290GICHLICP19 ] PR Lab Course in Inorganic Chemistry

Versionsauswahl
Workload Education level Study areas Responsible person Hours per week Coordinating university
5 ECTS B3 - Bachelor's programme 3. year Chemistry Christoph Topf 5 hpw Johannes Kepler University Linz
Detailed information
Pre-requisites VL Inorganic Chemistry II PR Lab Course in General Chemistry PR Lab Course in Preparative Organic Chemistry I

OR (particularly for Subject Chemistry):
PR Lab Course in General Chemistry VL Inorganic Chemistry II VO Fachdidaktik Chemie
Original study plan Bachelor's programme Chemistry and Chemical Technology 2025W
Learning Outcomes
Competences
Students completing the course will gain hands-on experience with research-guided laboratory experiments, fostering advanced, safe, and self-reliant practical skills in synthetic inorganic, organometallic, and materials chemistry. They will learn to manage air-, moisture-, and light-sensitive compounds and acquire the ability to safely handle corrosive or toxic substances. This training equips students with the competence to work responsibly and efficiently in chemical laboratory environments usually found in synthetic chemistry. Students will also gain the ability to evaluate and modify synthetic procedures found in original literature work and understand the scientific background of their lab work.
Skills Knowledge
The contents of the course will enable them to • Understand and implement safety protocols for handling chemicals and equipment (k2, k3, k4, k5) • Conduct and assess standard and advanced inorganic syntheses, including air- and moisture-sensitive reactions (k3, k4, k5) • Operate equipment such as spectrometers, Schlenk lines, advanced reaction apparatuses and glassware (k2, k3, k4) • Safely manage corrosive, flammable, toxic, or light-sensitive compounds (k2, k3, k4, k5) • Document experimental observations and analyze results (k1, k2, k4) • Troubleshoot reaction setups and to optimize conditions (k4, k5) • Apply theoretical knowledge to practical challenges (k1, k2, k3, k4) • Chemical safety principles • Synthesis of inorganic and organometallic compounds and their properties • Spectroscopic methods like NMR and IR • Schlenk techniques and performance of reactions under inert conditions • Experimental design for advanced synthetic reactions • Practical and theoretical main group and transition metal chemistry • Role of ligands and synthesis of ligands like Cp, phosphines, CO, amines, etc. • Documentation of lab work
Criteria for evaluation Entrance examination covering the necessary theoretical background, evaluation of the practical work actually carried out (including safety aspects and full documentation of all experiments in the lab protocols), as well as the result of a final oral examination.
Methods Research-guided chemical lab work including synthesis and product characterization with individual supervision by experienced assistants.
Language English
Study material Detailed lab instructions and required literature ressources will be provided on an individual basis.
Changing subject? No
Corresponding lecture TCBPAPRAOCH: PR Praktikum aus Anorganischer Chemie (6 ECTS)
On-site course
Maximum number of participants 10
Assignment procedure Direct assignment