 |
Detailed information |
Pre-requisites |
At least one of the following courses:
VL NMR Spectroscopy (Bachelor's programm Chemistry and Chemical Technology),
Modul Biomolecular NMR Spectroscopy (Bachelor's program Biological Chemistry),
VL Advanced NMR 1,
KV Advanded NMR 2, VL Understanding NMR Spectroscopy
|
Original study plan |
Master's programme Chemistry and Chemical Technology (CCT) 2025W |
Learning Outcomes |
Competences |
Students will understand and be able to apply, and explain how to use NMR spectrometers (practical and applied theory) and how to process and analyse NMR data.
|
|
Skills |
Knowledge |
More specifically, on completion of the course they will be able to
• follow NMR laboratory safety procedures. (k1, k2, k3)
• know, identify and operate the components of an NMR spectrometer. (k1, k2, k3)
• prepare NMR samples. (k1, k2, k3)
• know and apply the setup of routine NMR spectroscopic experiments. (k1, k2, k3)
• know and apply basic data processing. (k1, k2, k3, k4)
• identify, recognise and evaluate common errors. (k1, k2, k3, k4)
• know and apply the setup of multi-pulse and multi-dimensional experimental design. (k1, k2, k3)
• optimise acquisition and processing parameters. (k1, k2, k3, k4)
• know and apply advanced processing techniques. (k1, k2, k3)
|
Basic concepts and details of:
• Health and safety regulations for the operation of an NMR spectrometer
• Components of an NMR spectrometer
• State of the art experiments
• Operation of an NMR spectrometer
• Processing of NMR data
• Analysis of NMR data
|
|
Criteria for evaluation |
Practical performance, compliance with safety rules
|
Methods |
The course is highly interactive and includes demonstrations as well as guided operation of NMR spectrometers
|
Language |
English |
Study material |
Spectrometer manuals
Basic One and Two-Dimensional NMR Spectroscopy by Horst Friebolin
200 and More NMR Experiments: A Practical Course, Stefan Berger, Siegmar Braun
|
Changing subject? |
No |
Further information |
Instruments used: Bruker Avance III 300 (automatic sample changer), Bruker Avance III 500 (liquids and solids), demonstration on Bruker Avance III 700 with cryo-pobe
|
Corresponding lecture |
863STBCNMRP10: PR Practical NMR (2.4 ECTS)
|
|