Inhalt

[ 290OPCHOC1P18 ] PR (*)Lab Course in Preparative Organic Chemistry I

Versionsauswahl
Es ist eine neuere Version 2021W dieser LV im Curriculum Bachelorstudium Naturwissenschaftliche Grundlagen der Technik (NaWi-Tec) 2023W vorhanden.
(*) Leider ist diese Information in Deutsch nicht verfügbar.
Workload Ausbildungslevel Studienfachbereich VerantwortlicheR Semesterstunden Anbietende Uni
6 ECTS B2 - Bachelor 2. Jahr Chemie Norbert Müller 6 SSt Johannes Kepler Universität Linz
Detailinformationen
Anmeldevoraussetzungen (*)VL Organic Chemistry 1 PR Lab Course in General Chemistry
Quellcurriculum Bachelorstudium Chemistry 2018W
Ziele (*)Performing fundamental syntheses and characterisations of organic compounds .
Lehrinhalte (*)The course is divided into six consecutive sections devoted to particular reaction types. Section 1 deals with the preparative separation of organic compounds based on their acid/base properties and characterization by physical properties (Melting point, boiling point, refractive index and simple IR, MS and NMR spectra) Section 2 deals with nucleophilic aliphatic substitution reactions and safety issues. In section 3 the students will learn about properties and reactions of carbonyl compounds. Section 4 is devoted to electrophilic addition, elimination, reduction and oxidation reactions. In Section 5 reactions of aromatic compounds are in the focus of interest. Rearrangement and pericyclic reactions are the topic of the last section. In each section several practical assignments have to be performed in the lab under the supervision of experienced tutors and assistants. The students are required to adequately document their laboratory work in protocol books and take intermediate exams on safe laboratory procedures.
Beurteilungskriterien (*)Tests on safety issues and preparedness for the practical work

Practical performance including safe practice

Documentation of the results obtained (protocols)

Final comprehensive discussion of individual results

Lehrmethoden (*)Guided practical laboratory work
Abhaltungssprache Englisch
Literatur (*)
  • The organic chem lab survival manual : a student's guide to techniques / James W. Zubrick (Hudson Valley Community College)
  • Laboratory safety for chemistry students / Robert H. Hill, Jr., David C. Finster.
  • Practical Organic Chemistry - A student handbook of techniques; J. T. SharpI. GosneyA. G. Rowle
Lehrinhalte wechselnd? Nein
Sonstige Informationen (*)The course is held in parallel to "In-depth Fundamentals of Preparative Organic Chemistry" and the contents of both courses will be closely coordinated. It is highly recommended that the two courses course are attended in the same semester.
Äquivalenzen (*)290OCPCPOCP16: PR Praktikum aus präparativer Organischer Chemie I (7 ECTS)
Präsenzlehrveranstaltung
Teilungsziffer 10
Zuteilungsverfahren Direktzuteilung