Inhalt

[ 290OPCHOC1P18 ] PR Lab Course in Preparative Organic Chemistry I

Versionsauswahl
Es ist eine neuere Version 2021W dieser LV im Curriculum Bachelor's programme Fundamentals of Natural Sciences for Technology 2022W vorhanden.
Workload Education level Study areas Responsible person Hours per week Coordinating university
6 ECTS B2 - Bachelor's programme 2. year Chemistry Norbert Müller 6 hpw Johannes Kepler University Linz
Detailed information
Pre-requisites VL Organic Chemistry 1 PR Lab Course in General Chemistry
Original study plan Bachelor's programme Chemistry 2018W
Objectives Performing fundamental syntheses and characterisations of organic compounds .
Subject The course is divided into six consecutive sections devoted to particular reaction types. Section 1 deals with the preparative separation of organic compounds based on their acid/base properties and characterization by physical properties (Melting point, boiling point, refractive index and simple IR, MS and NMR spectra) Section 2 deals with nucleophilic aliphatic substitution reactions and safety issues. In section 3 the students will learn about properties and reactions of carbonyl compounds. Section 4 is devoted to electrophilic addition, elimination, reduction and oxidation reactions. In Section 5 reactions of aromatic compounds are in the focus of interest. Rearrangement and pericyclic reactions are the topic of the last section. In each section several practical assignments have to be performed in the lab under the supervision of experienced tutors and assistants. The students are required to adequately document their laboratory work in protocol books and take intermediate exams on safe laboratory procedures.
Criteria for evaluation Tests on safety issues and preparedness for the practical work

Practical performance including safe practice

Documentation of the results obtained (protocols)

Final comprehensive discussion of individual results

Methods Guided practical laboratory work
Language English
Study material
  • The organic chem lab survival manual : a student's guide to techniques / James W. Zubrick (Hudson Valley Community College)
  • Laboratory safety for chemistry students / Robert H. Hill, Jr., David C. Finster.
  • Practical Organic Chemistry - A student handbook of techniques; J. T. SharpI. GosneyA. G. Rowle
Changing subject? No
Further information The course is held in parallel to "In-depth Fundamentals of Preparative Organic Chemistry" and the contents of both courses will be closely coordinated. It is highly recommended that the two courses course are attended in the same semester.
Corresponding lecture 290OCPCPOCP16: PR Praktikum aus präparativer Organischer Chemie I (7 ECTS)
On-site course
Maximum number of participants 10
Assignment procedure Direct assignment