[ 863STBCNMRP10 ] PR Practical NMR

Es ist eine neuere Version 2018W dieser LV im Curriculum Master's programme Joint Master Programme Biological Chemistry 2018W vorhanden.
Workload Education level Study areas Responsible person Hours per week Coordinating university
2,4 ECTS M1 - Master's programme 1. year Chemistry Norbert Müller 2 hpw Johannes Kepler University Linz
Detailed information
Pre-requisites At least one of the following courses:

VL Spektroskopie und Strukturaufklärung I (Bachelor's programm Technical Chemistry), Modul Biomolecular NMR Spectroscopy (Bachelor's program Biological Chemistry), VL Advanced NMR 1, KV Advanded NMR 2

Original study plan Master's programme Joint Master Programme Biological Chemistry 2016W
Objectives Students learn how to use NMR spectrometers (hands-on and applied theory)
Subject NMR laboratory safety

Components of a spectrometer

Sample preparation

Structure of the spectrometer software

Setup for routine spectroscopy - basic acquisition

Basic processing

Recognizing errors

Setup of multi-pulse experiments and multi-dimensional

Optimizing acquisition and processing parameters

Advanced processing

Criteria for evaluation Practical performance, compliance with safety rules
Methods The course is highly interactive and includes demonstrations as well as guided operation of NMR spectrometers
Language English
Study material Spectrometer manuals

Basic One and Two-Dimensional NMR Spectroscopy by Horst Friebolin

200 and More NMR Experiments: A Practical Course, Stefan Berger, Siegmar Braun

Changing subject? No
Further information Instruments used: Bruker Avance III 300 (automatic sample changer), Bruker Avance III 500 (liquids and solids), demonstration on Bruker Avance III 700 with cryo-pobe
On-site course
Maximum number of participants 6
Assignment procedure Direct assignment