| Detailed information |
| Pre-requisites |
At least one of the following courses:
VL NMR Spectroscopy (Bachelor's programm Chemistry and Chemical Technology),
Modul Biomolecular NMR Spectroscopy (Bachelor's program Biological Chemistry),
VL Advanced NMR 1,
KV Advanded NMR 2
|
| Original study plan |
Master's programme Chemistry and Chemical Technology (CCT) 2023W |
| Objectives |
Students learn how to use NMR spectrometers (hands-on and applied theory)
|
| Subject |
NMR laboratory safety
Components of a spectrometer
Sample preparation
Structure of the spectrometer software
Setup for routine spectroscopy - basic acquisition
Basic processing
Recognizing errors
Setup of multi-pulse experiments and multi-dimensional
Optimizing acquisition and processing parameters
Advanced processing
|
| Criteria for evaluation |
Practical performance, compliance with safety rules
|
| Methods |
The course is highly interactive and includes demonstrations as well as guided operation of NMR spectrometers
|
| Language |
English |
| Study material |
Spectrometer manuals
Basic One and Two-Dimensional NMR Spectroscopy by Horst Friebolin
200 and More NMR Experiments: A Practical Course, Stefan Berger, Siegmar Braun
|
| Changing subject? |
No |
| Further information |
Instruments used: Bruker Avance III 300 (automatic sample changer), Bruker Avance III 500 (liquids and solids), demonstration on Bruker Avance III 700 with cryo-pobe
|
| Corresponding lecture |
863STBCNMRP10: PR Practical NMR (2.4 ECTS)
|
